Azobisisobutyronitrile → HCID 22618951, compound

HRID 2050784Notes

Reaction equation

CC[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH:9]([CH3:11])C.[C:12]([O:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH3:29])(=[O:16])[C:13]([CH3:15])=[CH2:14].C=CC1C=CC=CC=1.N(C(C)(C)C#N)=NC(C)(C)C#N>>[C:12]([O:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH3:29])(=[O:16])[C:13]([CH3:15])=[CH2:14].[CH2:11]=[CH:9][C:8]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

Reactant 4

HCID 6547Azobisisobutyronitrile

HCID 7501Styrene

HCID 8906Lauryl Methacrylate

HCID 234152-Methyldecane

Product 1

HCID 22618951HCID 22618951, compound

Procedure

In a 500 ml glass vessel equipped with a stirrer, a reflux condenser, and a nitrogen inlet pipe were placed 400 g of Isopar H, 160 g of lauryl methacrylate, 40 g of styrene, and 4 g of azobisisobutyronitrile and the polymerization was performed at 80° C. for 6 hours with stirring under a nitrogen stream to provide copoly(lauryl methacrylate-styrene) at a polymerization rate of 80%.

Workup

customIn a 500 ml glass vessel equipped with a stirrer, a reflux condenser, and a nitrogen inlet pipe

Sources & evidence

ORD record: ord-1007f6df36c146aeaed39703fa72bae6
Source dataset: uspto-grants-1991_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05015551

Reaction notes

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