3-Phenoxybenzyl alcohol → HCID 19833943, compound

HRID 2050801Notes

Reaction equation

HRID 2050801 reaction equation
[CH:1]1[C:11]2[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8][N:7]([C:16]#[N:17])[CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1.[O:18]([C:25]1[CH:26]=[C:27]([CH:30]=[CH:31][CH:32]=1)[CH2:28][OH:29])[C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1>>[CH:1]1[C:11]2[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8][N:7]([C:16](=[NH:17])[O:29][CH2:28][C:27]3[CH:30]=[CH:31][CH:32]=[C:25]([O:18][C:19]4[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=4)[CH:26]=3)[CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1

Participants

3

Reactant 2

HCID 262953-Phenoxybenzyl alcoholHCID 198338865,7-dihydro-6H-dibenz[c,e]azepine-6carbonitrile

Product 1

HCID 19833943HCID 19833943, compound

Procedure

starting from 5,7-dihydro-6H-dibenz[c,e]azepine-6-carbonitrile and m-phenoxybenzyl alcohol, there is obtained m-phenoxybenzyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate as a syrup, mass spectrum m/e:M+ 420 (14), 327 (13), 237 (35), 194 (100);

Sources & evidence

ORD record
ord-1ef417e1e5ce495da997e3bdb4515244
Source dataset
uspto-grants-1991_05
Patent number
US05015640

Reaction notes

Loading…