4-Chlorobenzyl alcohol → HCID 19834012, compound

HRID 2050802Notes

Reaction equation

HRID 2050802 reaction equation
[CH:1]1[C:11]2[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8][N:7]([C:16]#[N:17])[CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1.[Cl:18][C:19]1[CH:26]=[CH:25][C:22]([CH2:23][OH:24])=[CH:21][CH:20]=1>>[CH:1]1[C:11]2[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8][N:7]([C:16](=[NH:17])[O:24][CH2:23][C:22]3[CH:25]=[CH:26][C:19]([Cl:18])=[CH:20][CH:21]=3)[CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1

Participants

3

Reactant 2

HCID 133974-Chlorobenzyl alcoholHCID 198338865,7-dihydro-6H-dibenz[c,e]azepine-6carbonitrile

Product 1

HCID 19834012HCID 19834012, compound

Procedure

starting from 5,7-dihydro-6H-dibenz[c,e]azepine-6-carbonitrile and p-chlorobenzyl alcohol, there is obtained p-chlorobenzyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate, m.p. 103°-105° C.;

Sources & evidence

ORD record
ord-7cc8771e18854bc59bfac2217a56cd01
Source dataset
uspto-grants-1991_05
Patent number
US05015640

Reaction notes

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