Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Hexane | HCID 8058 | — |
| Reactant | HCID 19833992 | HCID 19833992 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 19833991 | HCID 19833991 | — |
Reaction Steps
1.0 g of benzyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate is dissolved in 1 ml of methanol. The solution is cooled to 0° C. and treated with 0.6 ml of a 5N alcoholic hydrochloric acid solution. After stirring at 0°-5° C. for ten minutes, 10 ml of n-hexane are added, the precipitated product is removed by filtration under suction, and there is obtained benzyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate hydrochloride, m.p. 90°-92° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05015640 |
|---|
| Source dataset | uspto-grants-1991_05 |
|---|
| ORD ID | ord-014c1c3751a74e55a64c0e84b280f990 |
|---|
| Source note | uspto-grants-1991_05 |
|---|
