Methacryloyl chloride → HCID 19833955, compound

HRID 2050844Notes

Reaction equation

[CH:1]1[C:11]2[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8][N:7]([C:16](=[NH:20])[O:17][CH2:18][CH3:19])[CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1.[CH3:21][C:22](=[CH2:26])[C:23](Cl)=[O:24]>>[CH3:26][C:22](=[CH2:21])[C:23]([N:20]=[C:16]([N:7]1[CH2:6][C:5]2[CH:4]=[CH:3][CH:2]=[CH:1][C:11]=2[C:10]2[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=2[CH2:8]1)[O:17][CH2:18][CH3:19])=[O:24]

Participants

Reactant 2

HCID 13528Methacryloyl chloride

HCID 19833914ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6carboximidate

Product 1

HCID 19833955HCID 19833955, compound

Procedure

starting from ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate and 2-methylacryloyl chloride, there is obtained ethyl N-(2-methylacryloyl)-5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate as a syrup, mass spectrum m/e: M+ 334 (20), 305 (16), 293 (7), 194 (100), 167 (29), 69 (21), 41 (30);

Sources & evidence

ORD record: ord-901d00c6ade74491b79b9d7551b66401
Source dataset: uspto-grants-1991_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05015640

Reaction notes

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