Benzyl chloroformate → HCID 54458906, compound

HRID 2050877Notes

Reaction equation

HRID 2050877 reaction equation
[CH:1]1[C:11]2[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8][N:7]([C:16](=[NH:20])[O:17][CH2:18][CH3:19])[CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1.Cl[C:22]([O:24][CH2:25][C:26]1[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=1)=[O:23]>>[CH2:25]([O:24][C:22]([N:20]=[C:16]([N:7]1[CH2:6][C:5]2[CH:4]=[CH:3][CH:2]=[CH:1][C:11]=2[C:10]2[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=2[CH2:8]1)[O:17][CH2:18][CH3:19])=[O:23])[C:26]1[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=1

Participants

3

Reactant 2

HCID 10387Benzyl chloroformateHCID 19833914ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6carboximidate

Product 1

HCID 54458906HCID 54458906, compound

Procedure

starting from ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6carboximidate and benzyl chloroformate, there is obtained ethyl N-benzyloxycarbonyl-5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate as a syrup, mass spectrum m/e:M+ 400 (6), 371 (6), 309 (32), 263 (20), 194 (35), 179 (15), 167 (27), 108 (12), 91 (100);

Sources & evidence

ORD record
ord-d27f4aefad7f445a9931bd964d78a227
Source dataset
uspto-grants-1991_05
Patent number
US05015640

Reaction notes

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