HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 178441985, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 4-(Trifluoromethyl)phenyl isocyanate | HCID 73768 | — |
| Reactant | HCID 178441986 | HCID 178441986 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 178441985 | HCID 178441985 | — |
Reaction Steps
To 5 g (20 mmole) of 3-t-butyl-5-(2-hydroxyethylthio)-1H-1,2,4-triazole in 50 ml of chloroform was added 0.1 g of triethylamine and 3.8 g (20 mmole) of 4-trifluoromethylphenylisocyanate. After refluxing for three hours, the mixture was concentrated in vacuo and crystallized from ether/hexane to give 3-t-butyl-5-(2-(4-trifluoromethylphenylcarbamoyloxy)-ethylthio)-1H-1,2,4-triazole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05015652 |
| Source dataset | uspto-grants-1991_05 |
| ORD ID | ord-c57afbab7f12482d88aa2456ed68a5f2 |
| Source note | uspto-grants-1991_05 |