2,6-Xylyl isocyanate → HCID 15172040, compound

Participants

Reaction Steps

To a solution of 1-phenylcyclopentyl amine (1.0 gm, 0.006 mole) in 30 ml of ethylacetate, 2,6-dimethylphenyl isocyanate (0.91 g; 0.006 mole) is added and the reaction mixture is stirred at room temperature for 20 hours. Volatiles are removed under reduced pressure and the residue is crystallized from ethylacetate-hexane yielding 1.65 g of N-(2,6-dimethylphenyl-N'-(1-phenylcyclopentyl) urea having a melting point of 227°-229° C.

Provenance & Evidence