Ammonia → HCID 15056980, compound

Participants

Reaction Steps

A mixture of 7.4 g of the compound from Example 3 and 50 ml of concentrated methanolic ammonia is left to stand at room temperature for 15 h. The solvent is stripped off, the residue is treated with active charcoal in hot ethyl acetate, and the mixture is filtered. The residue remaining after evaporation of the solvent is stirred with diethyl ether, filtered off with suction and dried.

Provenance & Evidence