Hydrochloric Acid → HCID 9837269, compound

HRID 2050918Notes

Reaction equation

HRID 2050918 reaction equation
Cl.[S:2]1[CH:6]=[CH:5][CH:4]=[C:3]1[CH:7]([NH:15][CH2:16][C:17]([NH2:19])=[O:18])[C:8]([O:10]C(C)(C)C)=[O:9]>C(O)(=O)C>[S:2]1[CH:6]=[CH:5][CH:4]=[C:3]1[CH:7]([NH:15][CH2:16][C:17]([NH2:19])=[O:18])[C:8]([OH:10])=[O:9]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 15056980HCID 15056980, compound

Product 1

HCID 9837269HCID 9837269, compound

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

Gaseous HCl is passed into a cooled solution of 2.4 g of the compound from Example 4 in 25 ml of glacial acetic acid until saturated. The mixture is allowed to reach room temperature while stirring. The precipitate which forms is filtered off with suction, washed with a little methanol and dried. Yield: 2.0 g melting point 206° C. (decomposition)

Workup

  1. customto reach room temperature
  2. filtrationThe precipitate which forms is filtered off with suction
  3. washwashed with a little methanol
  4. customdried

Sources & evidence

ORD record
ord-3444b27ffe1b413792534c108ba5e1be
Source dataset
uspto-grants-1991_05
Patent number
US05015659

Reaction notes

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