Hydrochloric Acid → HCID 19834258, compound

HRID 2050921Notes

Reaction equation

HRID 2050921 reaction equation
[ClH:1].[S:2]1[CH:6]=[CH:5][CH:4]=[C:3]1[CH2:7][C:8]([NH:10][NH:11][CH2:12][C:13]([O:15]C(C)(C)C)=[O:14])=[O:9]>C(O)(=O)C>[ClH:1].[S:2]1[CH:6]=[CH:5][CH:4]=[C:3]1[CH2:7][C:8]([NH:10][NH:11][CH2:12][C:13]([OH:15])=[O:14])=[O:9]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 86744773HCID 86744773, compound

Product 1

HCID 19834258HCID 19834258, compound

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

Gaseous HCl is passed into a stirred and cooled suspension of 3.2 g of the compound from Example 7 in 30 ml of glacial acetic acid until saturated. The mixture is then stirred for 1 h and the volatile fractions are removed in vacuo. The residue is recrystallized from ether.

Workup

  1. temperaturecooled
  2. stirringThe mixture is then stirred for 1 h
  3. customthe volatile fractions are removed in vacuo
  4. customThe residue is recrystallized from ether

Sources & evidence

ORD record
ord-c37ca67af57e405b8bf92174c19c9cd3
Source dataset
uspto-grants-1991_05
Patent number
US05015659

Reaction notes

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