HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Dihydroxy-2,2,6,6-tetramethylpiperidine → HCID 67827820, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Dihydroxy-2,2,6,6-tetramethylpiperidine | HCID 5395 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Sebacoyl chloride | HCID 66072 | — |
| Reactant | 1-Methoxy-2,2,6,6-tetramethyl-piperidin-4-ol | HCID 10997770 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 67827820 | HCID 67827820 | — |
Reaction Steps
Sebacoyl chloride is added to a mixture of 4-hydroxy-1-methoxy-2,2,6,6-tetramethylpiperidine, 4-hydroxyl-1-oxyl-2,2,6,6-tetramethylpiperidine, triethylamine and methylene chloride. The reaction mixture is worked up in the usual manner and purified by flash chromatography on silica gel to afford the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05015682 |
| Source dataset | uspto-grants-1991_05 |
| ORD ID | ord-2a179d901f994219952c061a6d4bc8d7 |
| Source note | uspto-grants-1991_05 |