Hydrogen Peroxide → HCID 14422495, compound

Participants

Reaction Conditions

Reaction Steps

To a suspension of 0.80 g of 6-chloro-2,3-dihydroimidazo[2,1-b]thiazole-5-sulfonamide-1-oxide in 10 ml of acetic acid is added 4 ml of 30% aqueous hydrogen peroxide solution followed by stirring for hour 100° C. After cooling, ice water is added to the reaction mixture to precipitate crystals. The crystals are collected by filtration, washed with water and dried to give 0.30 g of the title compound as colorless crystals. mp. 246°-247° C.

Provenance & Evidence