HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14422542, compound → Imidazo[1,5-a]pyridine-3-sulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14422542 | HCID 14422542 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | Imidazo[1,5-a]pyridine-3-sulfonamide | HCID 19832737 | 77.1% |
Reaction Steps
N-(t-Butyl)imidazo[1,5-a]pyridine-3-sulfonamide (1.0 g) is dissolved in 20 ml of trifluoroacetic acid and stirred for 14 days at room temperature. The mixture is concentrated under reduced pressure, and ether is added to the residue to precipitate crystals. The crystals are collected by filtration and dried to give 0.60 g of the title compound. mp. 179°-180° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05017212 |
| Source dataset | uspto-grants-1991_05 |
| ORD ID | ord-93a5aa6cf675491eb5055d96c4015b00 |
| Source note | uspto-grants-1991_05 |