HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 14552913, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Morpholine, 4-(chloroacetyl)- | HCID 74040 | — |
| Reactant | HCID 67946912 | HCID 67946912 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | HCID 14552913 | HCID 14552913 | 79.2% |
Reaction Steps
The procedure is as in Example 1, but starting with 2-(4-chlorophenyl)-5-trifluoromethyl-4-quinolone (2.9 g), 4-(2-chloroacetyl)morpholine (1.62 g) and anhydrous potassium carbonate (2.5 g) in 2-butanone (60 cc). After recrystallization in acetonitrile, 4-{[2-(4-chlorophenyl)-5-trifluoromethyl-4-quinolyl]oxyacetyl}morphline (3.2 g), m.p. 179° C., is isolated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05017576 |
| Source dataset | uspto-grants-1991_05 |
| ORD ID | ord-c3c1a2e5d1a94866a1c1e6b9c1b96dbe |
| Source note | uspto-grants-1991_05 |