Hydrochloric Acid → HCID 86744782, compound

HRID 2051289Notes

Reaction equation

HRID 2051289 reaction equation
[Cl:1][CH2:2][C:3](=[N:17][OH:18])[CH2:4][O:5][C:6]1[C:10]([N:11]2[CH2:16][CH2:15][O:14][CH2:13][CH2:12]2)=[N:9][S:8][N:7]=1.Cl>CCOCC>[ClH:1].[CH:3]([NH:17][CH2:2][C:3](=[N:17][OH:18])[CH2:4][O:5][C:6]1[C:10]([N:11]2[CH2:16][CH2:15][O:14][CH2:13][CH2:12]2)=[N:9][S:8][N:7]=1)([CH3:4])[CH3:2]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 73189422HCID 73189422, compound

Product 1

HCID 86744782HCID 86744782, compoundYield 89%

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent2×

Procedure

The oxime 4b (0.25 g) was dissolved in ether and ether saturated with HCl was introduced dropwise into the solution. The mixture was stirred for 10 minutes, filtered and dried in vacuo overnight. Yield: 89%. Anal. (C12H22N5O3SCl) C,H,N.

Workup

  1. filtrationfiltered
  2. customdried in vacuo overnight

Sources & evidence

ORD record
ord-08ec9a340ef044bfbccaf28971fdd969
Source dataset
uspto-grants-1991_05
Patent number
US05017618

Reaction notes

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