HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Dioxolane → HCID 20378047, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Dioxolane | HCID 12586 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 20378058 | HCID 20378058 | — |
| Product | HCID 20378047 | HCID 20378047 | 102.6% |
Reaction Steps
Hydrolysis of 9.0 g (0.039 mol) of diethyl 1,3-dioxane-2,2-dicarboxylate with 6.8 g of 50% aqueous sodium hydroxide as described in Example 2 for the dioxolane analog yielded 8.4 g (0.04 mol) 98% of the title compound as a white free flowing solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04182718 |
| Source dataset | uspto-grants-1980_01 |
| ORD ID | ord-c66742bc8374478fb937acb01e45c935 |
| Source note | uspto-grants-1980_01 |