HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 20378049, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Carbonate Ion | HCID 19660 | — |
| Reactant | 1,3-Diethyl 2-oxopropanedioate | HCID 69105 | — |
| Reactant | methyl 2-bromo-3-hydroxypropionate | HCID 11964350 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 20378049 | HCID 20378049 | — |
Reaction Steps
Diethyl ketomalonate 15 g (0.086 mol) and methyl 2-bromo-3-hydroxy-propionate (Example 5a)) were mixed and after returning to room temperature were treated with hexane (50 ml) and 18.6 g (0.134 mol) potassium carbonate. After 6 hours an additional 5.9 g of carbonate was added and the mixture stirred at 45° overnight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04182718 |
| Source dataset | uspto-grants-1980_01 |
| ORD ID | ord-893dd06d89e24067b08d88b1936011f1 |
| Source note | uspto-grants-1980_01 |