HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 2-[(2-pyridylmethyl)thio]-1H-naphth[2,3-d]imidazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 2-Pyridinemethanethiol | HCID 256071 | — |
| Reactant | 2-(methylthio)-1H-naphtho[2,3-d]imidazole | HCID 12872079 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-[(2-pyridylmethyl)thio]-1H-naphth[2,3-d]imidazole | HCID 22394184 | 81.7% |
Reaction Steps
0.45 g of 2-methylthio-1H-naphth[2,3-d]imidazole and 0.64 g of 2-mercaptomethylpyridine were heated for 40 hours under reflux in 10 ml of ethanol. 10 ml of water were added to the homogeneous solution and the precipitate formed was filtered off. 0.50 g of 2-[(2-pyridylmethyl)thio]-1H-naphth[2,3-d]imidazole having a m.p. of 170° was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04182766 |
| Source dataset | uspto-grants-1980_01 |
| ORD ID | ord-8cffeb46b0b14b5395d8e0e24fdbc492 |
| Source note | uspto-grants-1980_01 |