Isopropylamine → HCID 53918280, compound
Reaction equation
O=[CH:2][C@@H:3]([C@H:5]([C@@H:7]([CH2:9][OH:10])[OH:8])[OH:6])[OH:4].[CH:11]([NH2:14])([CH3:13])[CH3:12].[Cl:15][CH2:16][CH2:17][N:18]=[C:19]=[O:20]>>[Cl:15][CH2:16][CH2:17][NH:18][C:19]([N:14]([CH:11]([CH3:13])[CH3:12])[CH:9]1[O:10][CH2:2][C@@H:3]([OH:4])[C@H:5]([OH:6])[C@H:7]1[OH:8])=[O:20]Participants
4
Procedure
3.0 g of D-xylose, 2.5 g of isopropylamine and 2.5 g of 2-chloroethyl isocyanate are treated in the same manner as described in Example 5-(1). 4.0 g of 1-(2-chloroethyl)-3-isopropyl-3-D-xylopyranosylurea are thereby obtained as colorless caramel.
Sources & evidence
- ORD record
- ord-8f91fd57b28d41b08e3a2c613e22fe5f
- Source dataset
- uspto-grants-1980_01
- Patent number
- US04182757
Reaction notes
Loading…