HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(2-Naphthoxy)ethanol → 2-(2-Naphthyloxy)ethyl methanesulfonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(2-Naphthoxy)ethanol | HCID 7131 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 2-(2-Naphthyloxy)ethyl methanesulfonate | HCID 19004383 | — |
Reaction Steps
As described in Example 2, 13.5 g of 2-(2-naphthyloxy)ethanol in 400 ml of dichloromethane is reacted with 9.5 g of methanesulfonyl chloride in the presence of 11.4 g of triethylamine to give the product as tan crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04182776 |
| Source dataset | uspto-grants-1980_01 |
| ORD ID | ord-c77064d7c6a8497f83cbc3015820b13f |
| Source note | uspto-grants-1980_01 |