HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → 2-(2-Thienyl)ethyl methanesulphonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | 2-Thiopheneethanol | HCID 79400 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 2-(2-Thienyl)ethyl methanesulphonate | HCID 3047723 | — |
Reaction Steps
A mixture of 12.8 g of 2-(2-thienyl)ethanol and 20.2 g of triethylamine in 500 ml of dichloromethane is reacted with 12.6 g of methanesulfonyl chloride as described in Example 2 to give the product as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04182776 |
| Source dataset | uspto-grants-1980_01 |
| ORD ID | ord-0be8ae0e36d64558abd63297cdaa601c |
| Source note | uspto-grants-1980_01 |