HRID2051895

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID14797

Potassium hydroxide

HKO

HCID13079686

Ethyl 4-{[2-(thiophen-2-yl)ethyl]amino}benzoate

C15H17NO2S

PRODUCTS

产物

HCID13079685

4-{[2-(Thiophen-2-yl)ethyl]amino}benzoic acid

C13H13NO2S

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

A mixture of 29.7 g of ethyl p-[2-(2-thienyl)ethylamino]benzoate and 29 g of potassium hydroxide in 200 ml of 95% ethanol is refluxed for 3 hours. The mixture is worked up as described in Example 4 to give the product, mp 161°-163° C.

WORKUP

后处理

temperatureis refluxed for 3 hours
customto give the product, mp 161°-163° C.