HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 23468298, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | Ethanol, 2-(1-naphthalenyloxy)- | HCID 69734 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 23468298 | HCID 23468298 | — |
Reaction Steps
To a solution of 18.8 g of 2-(1-naphthyloxy)ethanol and 15.1 g of triethylamine in 425 ml of dichloromethane is added 12.6 g of methanesulfonyl chloride as described in Example 1 to give the product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04182776 |
| Source dataset | uspto-grants-1980_01 |
| ORD ID | ord-0b2e7f0800a84f2890856279d22c5537 |
| Source note | uspto-grants-1980_01 |