Triethylamine → HCID 23468298, compound

HRID 2051896Notes

Reaction equation

HRID 2051896 reaction equation
[C:1]1([O:11][CH2:12][CH2:13][OH:14])[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][CH:2]=1.C(N(CC)CC)C.[CH3:22][S:23](Cl)(=[O:25])=[O:24]>ClCCl>[CH3:22][S:23]([O:14][CH2:13][CH2:12][O:11][C:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][CH:2]=1)(=[O:25])=[O:24]

Participants

5

Reactant 3

HCID 8471TriethylamineHCID 31297Methanesulfonyl chlorideHCID 69734Ethanol, 2-(1-naphthalenyloxy)-

Product 1

HCID 23468298HCID 23468298, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

To a solution of 18.8 g of 2-(1-naphthyloxy)ethanol and 15.1 g of triethylamine in 425 ml of dichloromethane is added 12.6 g of methanesulfonyl chloride as described in Example 1 to give the product.

Workup

  1. customto give the product

Sources & evidence

ORD record
ord-0b2e7f0800a84f2890856279d22c5537
Source dataset
uspto-grants-1980_01
Patent number
US04182776

Reaction notes

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