HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzocaine → HCID 23468280, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzocaine | HCID 2337 | — |
| Reactant | HCID 23468298 | HCID 23468298 | — |
| Solvent | Hexamethylphosphoramide | HCID 12679 | — |
| Product | HCID 23468280 | HCID 23468280 | — |
Reaction Steps
A solution of 29.1 g of 2-(1-naphthyloxy)ethanol O-methanesulfonate and 33 g of ethyl p-aminobenzoate in 100 ml of hexamethylphosphoramide is heated at 100° C. for 16 hours. The solution is worked up as described in Example 3 to give the product. Recrystallization gives crystals, mp 124°-127° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04182776 |
| Source dataset | uspto-grants-1980_01 |
| ORD ID | ord-0886274feb0e457ba442d8956a70d872 |
| Source note | uspto-grants-1980_01 |