HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 23468289, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 23468280 | HCID 23468280 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 23468289 | HCID 23468289 | — |
Reaction Steps
A solution of 12 g of ethyl p-[2-(1-naphthyloxy)-ethylamino]benzoate and 15.8 g of potassium hydroxide in 100 ml of 95% ethanol is refluxed for 3 hours. The solution is diluted with 75 ml of water and acidified with concentrated hydrochloric acid. The solid is filtered, washed with 50% ethanol and with water. Recrystallization from ethanol gives the product as crystals, mp 193°-194° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04182776 |
| Source dataset | uspto-grants-1980_01 |
| ORD ID | ord-15f21c0bd96548e2b41579e910a1934f |
| Source note | uspto-grants-1980_01 |