HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 20378402, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Ethyl p-{[2-(2,4-dichlorophenoxy)ethyl]amino}benzoate | HCID 20378376 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 20378402 | HCID 20378402 | — |
Reaction Steps
A solution of 15 g of ethyl p-{[2-(2,4-dichlorophenoxy)ethyl]amino}benzoate and 15 g of potassium hydroxide in 200 ml. of 95% ethanol is refluxed for 3 hours. The solution is cooled, diluted with water, acidified with concentrated hydrochloric acid and filtered. The solid is recrystallized from ethanol to give crystals, mp 203°-205° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04182776 |
| Source dataset | uspto-grants-1980_01 |
| ORD ID | ord-6896fc87fd7a419380be695fe390ff4a |
| Source note | uspto-grants-1980_01 |