HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzocaine → HCID 20378380, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzocaine | HCID 2337 | — |
| Reactant | HCID 20378398 | HCID 20378398 | — |
| Solvent | Hexamethylphosphoramide | HCID 12679 | — |
| Product | HCID 20378380 | HCID 20378380 | — |
Reaction Steps
A solution of 13.6 g of 6-(phenoxy)-1-hexanol O-methanesulfonate and 16.5 g of ethyl p-aminobenzoate in 75 ml of hexamethylphosphoramide is heated at 110° C. for 16 hours. The product is isolated as described in Example 3 to give crystals. Recrystallization from ethanol gives crystals, mp 105°-108° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04182776 |
| Source dataset | uspto-grants-1980_01 |
| ORD ID | ord-af58c6b97b374320950b1c9ab218e388 |
| Source note | uspto-grants-1980_01 |