HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 20378394, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 131711674 | HCID 131711674 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 20378394 | HCID 20378394 | — |
Reaction Steps
A solution of 2.6 g of ethyl p-[2-(4-fluorophenoxy)propylaminobenzoate in 100 ml of 95% ethanol containing 2.7 g of potassium hydroxide was heated to reflux for 2 hours. The reaction was cooled, diluted with 100 ml of water and neutralized with 37% hydrochloric acid. The solid was collected and dried giving a white solid which was dissolved in 25 ml of chloroform and diluted with 1 ml of hexane giving a solid with a m.p. 171°-172° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04182776 |
| Source dataset | uspto-grants-1980_01 |
| ORD ID | ord-7dfb2948814a4c8285f2bfc886bd03d3 |
| Source note | uspto-grants-1980_01 |