Sulfuric Acid → N-(1-methylnonyl)acrylamide

HRID 2051936Notes

Reaction equation

[C:1](#[N:4])[CH:2]=[CH2:3].[CH2:5]=[CH:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14].C1C2NC3C(=CC=CC=3)SC=2C=CC=1.S(=O)(=O)(O)[OH:30]>>[CH3:5][CH:6]([NH:4][C:1](=[O:30])[CH:2]=[CH2:3])[CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14]

Participants

Reactant 4

HCID 1118Sulfuric Acid

HCID 7108Phenothiazine

HCID 7855Acrylonitrile

HCID 133811-Decene

Product 1

HCID 3018347N-(1-methylnonyl)acrylamide

Procedure

Following a procedure analogous to that of Example 1, treat acrylonitrile with 1-decene in the presence of phenothiazine and 83% sulfuric acid to obtain the title product.

Sources & evidence

ORD record: ord-68f5833136fb49a2ab4b0908d2a102a0
Source dataset: uspto-grants-1980_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04182790

Reaction notes

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