Indacrinone → 76698-88-9

HRID 2052060Notes

Reaction equation

HRID 2052060 reaction equation
[O:1]=[C:2]1[C:10]2[C:5](=[CH:6][C:7]([O:13][CH2:14][C:15]([OH:17])=[O:16])=[C:8]([Cl:12])[C:9]=2[Cl:11])[CH2:4][C:3]1([CH3:24])[C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1.C(=O)(O)[O-].[Na+:29]>O>[O:1]=[C:2]1[C:10]2[C:5](=[CH:6][C:7]([O:13][CH2:14][C:15]([O-:17])=[O:16])=[C:8]([Cl:12])[C:9]=2[Cl:11])[CH2:4][C:3]1([CH3:24])[C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1.[Na+:29]

Participants

4

Reactant 2

HCID 42266IndacrinoneHCID 516892Sodium Bicarbonate

Product 1

HCID 8673578076698-88-9

Reagents, catalysts & solvents 1

HCID 962WaterSolvent2×

Procedure

(1-Oxo-2-methyl-2-phenyl-6,7-dichloro-5-indanyloxy)acetic acid (1 gm.) is treated with sodium bicarbonate (0.25 gm.) in water (10 ml.) and the mixture stirred and heated to effect solution. The solution is diluted with water to a volume of 50 ml. and sterilized by autoclaving at 120° C. for one hour.

Workup

  1. temperatureheated

Sources & evidence

ORD record
ord-268d18d5de8a417895da7d4e40b9b70f
Source dataset
uspto-grants-1980_01
Patent number
US04182764

Reaction notes

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