HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 178503857, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | N-(1-methylimidazol-2-yl)-N'-phenylthiourea | HCID 20378498 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178503857 | HCID 178503857 | — |
Reaction Steps
A solution of 3.0 g (0.013 mole) of N-(1-methylimidazol-2-yl)-N'-phenylthiourea in 50 ml of methanol is added 2.13 g (0.015 mole) of methyl iodide. The solution is heated under reflux for 2 hr, the solvent is evaporated and the residue is recrystallized from acetone-ether to give methyl N-(1-methylimidazol-2-yl)-N'-phenylcarbamimidothioate hydroiodide; m.p. 115°-118° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04182865 |
| Source dataset | uspto-grants-1980_01 |
| ORD ID | ord-400c710788dd4492a1beb4781e19078d |
| Source note | uspto-grants-1980_01 |