反应详情

Saturated with anhydrous ammonia a solution containing 23 g (0.1 mole) of 3-phenoxybenzoyl chloride and 250 ml of AR chloroform. Continued stirring for 30 min., chilled to 0° and filtered. The product was pulverised, triturated in cold water and oven-dried to give 21.3 g, m.p. 127°-128°.

1. temperaturechilled to 0°
2. filtrationfiltered
3. customtriturated in cold water
4. customoven-dried
5. customto give 21.3 g, m.p. 127°-128°