HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ammonia → 3-Phenoxybenzamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ammonia | HCID 222 | — |
| Edukt | 3-Phenoxybenzoyl chloride | HCID 2760341 | — |
| Lösungsmittel | Chloroform | HCID 6212 | — |
| Produkt | 3-Phenoxybenzamide | HCID 16618625 | — |
Reaktionsschritte
Saturated with anhydrous ammonia a solution containing 23 g (0.1 mole) of 3-phenoxybenzoyl chloride and 250 ml of AR chloroform. Continued stirring for 30 min., chilled to 0° and filtered. The product was pulverised, triturated in cold water and oven-dried to give 21.3 g, m.p. 127°-128°.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04182881 |
| Quelldatensatz | uspto-grants-1980_01 |
| ORD ID | ord-a39fde958b4e4272b8722604470a7011 |
| Quellennotiz | uspto-grants-1980_01 |