HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 4-Butoxybenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 4-Butoxybenzoic acid | HCID 72971 | — |
| Product | 4-Butoxybenzoyl chloride | HCID 118561 | — |
Reaction Steps
Heated at reflux a solution of 75 g (0.39 mole) of 4-n-butoxybenzoic acid in 250 ml of thionyl chloride for 3 hrs. Removed by vacuum distillation the excess thionyl chloride to give 84 g of a brown colored liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04182881 |
| Source dataset | uspto-grants-1980_01 |
| ORD ID | ord-40f68a5341a644bc90103b090e74f8ba |
| Source note | uspto-grants-1980_01 |