HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → 4-butoxybenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 4-Butoxybenzoyl chloride | HCID 118561 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 4-butoxybenzamide | HCID 4306315 | — |
Reaction Steps
Chilled to 20°, a solution of 84 g (0.39 mole) of a solution of 4-n-butoxybenzoyl chloride in 700 ml of AR chloroform, then saturated with anhydrous ammonia. The mixture was stirred for 20 min. to 0°, then the white precipitate collected, washed with cold water and oven-dried to 60° to give 76 g, m.p. shrinks 160°, melts 162°-164°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04182881 |
| Source dataset | uspto-grants-1980_01 |
| ORD ID | ord-1506df6ddfcf4c86b4c1a0c86eccd7f3 |
| Source note | uspto-grants-1980_01 |