HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → 4-Phenylbenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 4-Phenylbenzoyl chloride | HCID 84151 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 4-Phenylbenzamide | HCID 602506 | — |
Reaction Steps
A mixture of 27 g (0.12 mole) of 4-biphenylcarbonyl chloride and 300 ml of AR chloroform was saturated with anhydrous ammonia while maintaining a temperature of 20°. Following the 20 min. addition the white precipitate was collected, washed with cold water and oven-dried (60°) to give 23.5 g, m.p. shrinks 228°, melts 230°-233°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04182881 |
| Source dataset | uspto-grants-1980_01 |
| ORD ID | ord-1e78e7e665dc42208b0c1debf78051be |
| Source note | uspto-grants-1980_01 |