HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → 2,4-Dimethylbenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 2,4-Dimethylbenzoyl chloride | HCID 140867 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 2,4-Dimethylbenzamide | HCID 12862392 | — |
Reaction Steps
Saturated with anhydrous ammonia, a solution of 50 g (0.3 mole) of 2,4-dimethylbenzoyl chloride and 500 ml of AR chloroform, while maintaining a temperature of 15°. Stirred for 20 min., then filtered, washed with cold distilled water and oven-dried at 60° to give 29.1 g, m.p. 184°-186°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04182881 |
| Source dataset | uspto-grants-1980_01 |
| ORD ID | ord-95271637ff844c6bb7b4599e8eba72f1 |
| Source note | uspto-grants-1980_01 |