HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4,6-Trimethylbenzoic acid → 2,4,6-Trimethylbenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4,6-Trimethylbenzoic acid | HCID 10194 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | 2,4,6-Trimethylbenzoyl chloride | HCID 97038 | — |
Reaction Steps
A solution of 50 g (0.3 mole) of 2,4,6-trimethylbenzoic acid and 150 ml of thionyl chloride was heated at reflux for 3 hrs. The excess thionyl cloride was removed by vacuum distillation to give 53.5 g of an amber colored liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04182881 |
| Source dataset | uspto-grants-1980_01 |
| ORD ID | ord-3f784c36f2e348d18b60c7396f787c09 |
| Source note | uspto-grants-1980_01 |