HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formic Acid → HCID 20378789, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formic Acid | HCID 284 | — |
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Reactant | 2,4,6-trimethylbenzamide | HCID 246686 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 20378789 | HCID 20378789 | — |
Reaction Steps
A suspension of 21 g (0.13 mole) of 2,4,6-trimethylbenzamide and 26.8 g (0.13 mole) of phosphorus pentachloride in 200 ml of AR carbon tetrachloride was heated at 70° for 30 min. The solution was cooled to 30° and 6.1 g (0.13 mole) of 97% formic acid added dropwise. Stirred for another 20 min., then filtered, washed with AR carbon tetrachloride and air-dried to give 20.5 g, m.p. 109°-110°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04182881 |
| Source dataset | uspto-grants-1980_01 |
| ORD ID | ord-1ce8683b35fe4625a85aff29ac4e6f07 |
| Source note | uspto-grants-1980_01 |