HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Isoxazolamine, 5-(1,1-dimethylethyl)- → N'-(5-tert-Butyl-1,2-oxazol-3-yl)-N-methyl-N-prop-2-en-1-ylurea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Isoxazolamine, 5-(1,1-dimethylethyl)- | HCID 171473 | — |
| Reactant | 51493-18-6 | HCID 22155864 | — |
| Product | N'-(5-tert-Butyl-1,2-oxazol-3-yl)-N-methyl-N-prop-2-en-1-ylurea | HCID 13373599 | 90.5% |
Reaction Steps
Using 3-amino-5-t-butylisoxazole and N-allyl-N-methylcarbamoyl chloride, the reaction is effected as in Example 1, whereby 1-allyl-1-methyl-3-(5-t-butyl-3-isoxazolyl)urea is obtained. Yield is 90.5%. Melting point is 90.0° to 91.0° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04183856 |
| Source dataset | uspto-grants-1980_01 |
| ORD ID | ord-dfc7a98445cd4c4da4b2bcaa11a26b57 |
| Source note | uspto-grants-1980_01 |