HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylcarbamoyl chloride → N'-(5-tert-Butyl-1,2-oxazol-3-yl)-N,N-diethylurea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylcarbamoyl chloride | HCID 6916 | — |
| Reactant | 3-Isoxazolamine, 5-(1,1-dimethylethyl)- | HCID 171473 | — |
| Product | N'-(5-tert-Butyl-1,2-oxazol-3-yl)-N,N-diethylurea | HCID 20377185 | 98.2% |
Reaction Steps
Using 3-amino-5-t-butylisoxazole and N,N-diethylcarbamoyl chloride, the reaction is effected as in Example 1, whereby 1,1-diethyl-3-(5-t-butyl-3-isoxazolyl)urea is obtained. Yield is 98.2%. Melting point is 122.0° to 123.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04183856 |
| Source dataset | uspto-grants-1980_01 |
| ORD ID | ord-4b12ad8014da4edb9b742bbdc996555c |
| Source note | uspto-grants-1980_01 |