Hydrochloric Acid → HCID 12897302, compound

HRID 2052588Notes

Reaction equation

HRID 2052588 reaction equation
[Cl:1][C:2]1[C:7]([NH:8][C:9](=[O:15])[C:10]([O:12]CC)=[O:11])=[CH:6][CH:5]=[CH:4][C:3]=1[NH:16][C:17](=[O:23])[C:18]([O:20]CC)=[O:19].Cl>[OH-].[Na+].O>[Cl:1][C:2]1[C:7]([NH:8][C:9](=[O:15])[C:10]([OH:12])=[O:11])=[CH:6][CH:5]=[CH:4][C:3]=1[NH:16][C:17](=[O:23])[C:18]([OH:20])=[O:19]

Participants

5

Reactant 2

HCID 313Hydrochloric AcidHCID 12897301HCID 12897301, compound

Product 1

HCID 12897302HCID 12897302, compound

Reagents, catalysts & solvents 2

HCID 962WaterSolventHCID 14798Sodium HydroxideSolvent

Procedure

Diethyl N,N'-(2-chloro-m-phenylene)dioxamate (0.50 gram) is heated at reflux in 1.0N aqueous sodium hydroxide (10 ml.) for one hour. The reaction mixture is diluted with water (15 ml.). Concentrated hydrochloric acid is added to pH 3 and the solid product collected by filtration (0.27 grams, M.P. >320°).

Workup

  1. filtrationthe solid product collected by filtration (0.27 grams, M.P. >320°)

Sources & evidence

ORD record
ord-5420e6a1d4d34ce2a6eb62ccafff5efc
Source dataset
uspto-grants-1980_01
Patent number
US04186127

Reaction notes

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