HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acrylic Acid → HCID 86602575, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acrylic Acid | HCID 6581 | — |
| Reactant | Propylene glycol methyl ether acetate | HCID 7946 | — |
| Reactant | 2-Hydroxyethyl Methacrylate | HCID 13360 | — |
| Reactant | tert-Butyl acrylate | HCID 15458 | — |
| Catalyst | Azobisisobutyronitrile | HCID 6547 | — |
| Product | HCID 86602575 | HCID 86602575 | 210.1% |
Reaction Steps
12 g of t-butylacrylate, 5 g of acrylic acid, 3 g of 2-hydroxyethylmethacrylate and 0.4 g of AIBN were added to 200 g of PGMEA, and were then polymerized at 60° C. for 8 hours. After completion of the polymerization, the mixture was precipitated in ether, filtered, and dried in vacuo to yield 16 g of t-butylacrylate-acrylic acid-2-hydroxyethylmethacrylate copolymer, as a white solid, represented by Formula 2 below:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07326525B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-de12a85a646140a19959027baeac01d4 |
| Source note | uspto-grants-2008_02 |