HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 69224673, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Bromopropiophenone | HCID 16452 | — |
| Reactant | HCID 68809102 | HCID 68809102 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 69224673 | HCID 69224673 | — |
Reaction Steps
A mixture of 2-bromo-1-phenylpropan-1-one (3 mmol), N-(2-hydroxy-phenyl acetyl)piperazine hydrochloride (2.5 mmol) and K2CO3 (8.75 mmol) in 30 ml of DMF was treated according to the general preparation 2 to give compound (IV-18), 0.65 g (67%), M+ 353.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07326710B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-37dc5b85e5034c63a36743aded7ba5c3 |
| Source note | uspto-grants-2008_02 |