HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 131726749, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | (2,4-difluorophenyl)methanesulfonyl Chloride | HCID 2761455 | — |
| Reactant | 1-Phenyl-2-(piperazin-1-yl)ethan-1-one--hydrogen chloride (1/2) | HCID 23080512 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 131726749 | HCID 131726749 | — |
Reaction Steps
A mixture of 2,4-difluorobenzylsulfonylchloride (3.5 mmol), N-phenacyl piperazine dihydrochloride (3 mmol), and K2CO3 (10.5 mmol) in 30 ml of DMF was treated according to the general preparation 2 to give compound (IV-22), 0.81 g (71%), M+ 412.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07326710B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-b7a1702e17a248c981400a4ce97ed0ca |
| Source note | uspto-grants-2008_02 |