HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 69224686, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | N-Benzyl-2-chloroacetamide | HCID 96233 | — |
| Reactant | HCID 52983664 | HCID 52983664 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 69224686 | HCID 69224686 | — |
Reaction Steps
A mixture of chloroacetylbenzylamine (3.06 mmol), N-(4-methoxyphenacyl) piperazine dihydrochloride (3 mmol, prepared by using the general preparation 1) and K2CO3 (10.5 mmol) in 30 ml of DMF was treated according to the general preparation 2 to give compound (IV-28), 0.86 g (74%), M+ 381.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07326710B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-6097bb3e4cb4461bb48b035b8396fba2 |
| Source note | uspto-grants-2008_02 |