HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylboronic Acid → HCID 68497053, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylboronic Acid | HCID 66827 | — |
| Reactant | HCID 68494747 | HCID 68494747 | — |
| Product | HCID 68497053 | HCID 68497053 | — |
Reaction Steps
The chloro thiazole (114)(80 mg, 0.24 mmol) was coupled to phenylboronic acid (32mg, 0.26 mmol) using Method E, except that the reaction mixture was heated for a total of 4 h. The crude residue was purified by column chromatography eluting with 25% EtOAc in heptane to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07326732B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-ba81a6fc5c6c437796eb0673efe824d1 |
| Source note | uspto-grants-2008_02 |