HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Dichlorophenylboronic acid → HCID 59654629, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Dichlorophenylboronic acid | HCID 2734331 | — |
| Reactant | HCID 59654644 | HCID 59654644 | — |
| Product | HCID 59654629 | HCID 59654629 | — |
Reaction Steps
The pyridyl bromide (77)(44 mg, 0.12 mmol) was coupled to 3,5-dichloro-phenylboronic acid (20 mg, 0.10 mmol) using Method E. During this reaction, hydrolysis occurred. The residue was extracted using Work-up E1 to give the acid. The solid was further purified by preparative HPLC to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07326732B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-690edc3264094bfd8fba9f4163a776f6 |
| Source note | uspto-grants-2008_02 |